Synthesis and spectra of some ²h-, ¹³c-, and ¹⁵n-labeled isomers of 1, 3, 3-trinitroazetidine and 3, 3-dinitroazetidinium nitrate

Authors

M. D. Coburn, Los Alamos National Laboratory
M. A. Hiskey, Los Alamos National Laboratory
J. C. Oxley, University of Rhode Island
J. L. Smith, University of Rhode Island
W. Zheng, University of Rhode Island
E. Rogers, University of Rhode Island

Document Type

Article

Date of Original Version

1-1-1998

Abstract

The title compounds were synthesized by utilizing appropriately labeled starting materials and reagents according to literature procedures.1, 2 The products were characterized by NMR and mass spectral analysis. Unequivocal assignments of all NMR chemical shifts of the unlabeled title compounds and their intermediate precursors were facilitated by the NMR spectra of the labeled compounds along with carbon-hydrogen correlation experiments. © 1998 Taylor & Francis Group, LLC.

Publication Title, e.g., Journal

Journal of Energetic Materials

Volume

16

Issue

2-3

Citation/Publisher Attribution

Coburn, M. D., M. A. Hiskey, J. C. Oxley, J. L. Smith, W. Zheng, and E. Rogers. "Synthesis and spectra of some ²h-, ¹³c-, and ¹⁵n-labeled isomers of 1, 3, 3-trinitroazetidine and 3, 3-dinitroazetidinium nitrate." Journal of Energetic Materials 16, 2-3 (1998): 73-99. doi: 10.1080/07370659808217506.