Document Type

Article

Date of Original Version

1-1-2017

Abstract

N,N-dimethylformamide sulfur trioxide complex (DMF-SO3) has been investigated as an electrolyte additive for LiNi0.5Mn1.5O4/graphite cells cycled to 4.8 V. Addition of 0.1% DMF-SO3 to 1.2 M LiPF6 in EC/EMC (3/7, v/v) standard electrolyte (STD) results in a significant improvement in the capacity retention and coulombic efficiency of LiNi0.5Mn1.5O4/graphite cells after 50 cycles at 45◦C. Ex-situ surface analysis of the electrodes after cycling has been conducted via scanning electron microscopy (SEM), transmission electron microscopy (TEM), X-ray photoelectron spectroscopy (XPS), and infrared spectroscopy with attenuated total reflectance (IR-ATR). The surface analysis suggests that a uniform interfacial film is formed on the LiNi0.5Mn1.5O4 surface composed of the decomposition products of DMF-SO3. The novel cathode surface films passivates the surface at high potential leading to the improved electrochemical performance.

Publication Title, e.g., Journal

Journal of the Electrochemical Society

Volume

164

Issue

13

Creative Commons License

Creative Commons License
This work is licensed under a Creative Commons Attribution-Noncommercial-No Derivative Works 4.0 License.

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